Tạp chí Khoa học, T. 14, S. 9 (2017)

Cỡ chữ:  Nhỏ  Vừa  Lớn

Preparation of some new schiff bases from 5-nitrovanillin

Duong Quoc Hoan, Nguyen Thi Hanh, Truong Minh Luong, Hoang Thi Nhu Quynh, Nguyen Hien

Tóm tắt

A series of Schiff bases were synthesized successfully based on the condensation reaction between 5-nitrovanillin and aromatic amines in moderate and high yields. The condensation underwent better in DCM solvent, acetic acid catalyst and anhydrous MgSO4 as a drying agent and increased the yield up to 100 %.These new Schiff bases were determined with 1H, 13C NMR spectral analysis and compound 3a was studied further HSQC, HMBC, NOSY and MS spectra. The C=N bond exists in E conformation.

Toàn văn: PDF

Tạp chí của Trường Đại học Sư phạm Thành phố Hồ Chí Minh ; ISSN: 1859 -3100